KS ANALYTICAL SYSTEMS

Tag: D8

  • Bruker D4 Endeavor on its way out

    Bruker D4 Endeavor on its way out

    The D4 Endeavor fits in a unique niche in the XRD world. It’s basically the same thing as a Bruker D8, but built into a very compact cabinet with a large autosampler on top. These machines see heavy use in the cement, pharmaceuticals, and aluminum industries among others. Today we have one headed out to a new home. It started life in the pharmaceutical world, but had light use so it was a great candidate for refurbishment.

  • KS Analytical Systems now offers new Bruker XRD and XRF hardware

  • Energy-dispersive detector systems for XRD applications

    Energy-dispersive detector systems for XRD applications

    Energy resolution

    • 140eV under ideal conditions.
    • All KB peaks eliminated electronically.
    • W LA1 (8.40 KeV) lines eliminated from Cu KA1,2 (8.04 KeV) scans even with thoroughly contaminated tubes.
    • Common fluorescence energies (i.e. Fe when Cu tube anodes are used) are greatly reduced. (Brehmstralung effects are impossible to remove completely)
    • Most PSD detectors offer no better than 650eV. This allows for a great deal of fluorescence energy to pass as well as W LA1 from older Cu tubes.

    Low angle scatter

    • The detector mounts in place of the traditional scintillation counter allowing for use of automated variable (motorized) or interchangeable aperture slits to control angular resolution. Scans starting from 0.5 degrees 2? are possible with the proper slit arrangement just as they are with the scintillation counter. The user controls the intensity vs angular resolution of the scan based upon the ideal conditions for their work rather than the limitations of the hardware.
    • Position sensitive detectors are wide open by design which necessitates knife edges over the sample and additional mechanical aperture plates to block air scatter at low angles. Closing off the detector limits the useable channels and reduces the benefit of these detectors dramatically.

    Truly zero maintenance design

    • No delays – The detector is ready to collect data almost as soon as power is applied.
    • No external cooling – Air backed Peltier cooling eliminates the need for water circulation and/or liquid nitrogen.
    • Zero maintenance vacuum design eliminates reliance on an ion pump/backup battery.
    • 12-month warranty against hardware failure under normal use.

    Versatility

    • The Digital Pulse Processor (DPP) includes a usb interface allowing for adjustment and refinement should they be necessary for a particular application. With optional software, full quantitative EDXRF analysis can be performed.

    The detector can be set for any common XRD anode (energy) easily. Multiple energies may even be configured to allow for use with various anodes without the need for additional hardware. We specialize in Siemens (now Bruker) XRD and WD-XRF instrumentation and have installation kits ready for the D500, D5000 and D5005. The output is a standard BNC cable with a 5V square pulse output which is standard across every manufacturer we’ve worked with. Kevex and Thermo Si(Li) detectors used this same output.

    Please contact KS Analytical Systems for a quote.